Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: Chemical structure of aflatoxin B 1 (AFB 1 ), aflatoxin B 2 (AFB 2 ), aflatoxin G 1 (G 1 ), aflatoxin G 2 (AFG 2 ), 3-acetyldeoxynivalenol (3-ADON), 15-acetyldeoxynivalenol (15-ADON), deoxynivalenol (DON), deoxynivalenol-3-glucoside (DON-3-G), moniliformin (MON), nivalenol (NIV), and zearalenone (ZEA).

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques:

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: Optimized ESI-MS and ESI-MS/MS parameters and monitored transition reactions for the analyzed mycotoxins.

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques:

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: LC-ESI-MS/MS chromatograms of mycotoxins from maize extract spiked at 8 μg kg -1 for AFB 1 , 2 μg kg -1 for AFG 1 and AFB 2 , 1 μg kg -1 for AFG 2 , 100 μg kg -1 for 3-ADON, FB 2 and MON, 40 μg kg -1 for 15-ADON and NIV, 168 μg kg -1 for DON, 50 μg kg -1 for DON-3-G, 32.4 μg kg -1 for ENNA, 36 μg kg -1 for ENNA 1 , 28 μg kg -1 for ENNB, 30.4 μg kg -1 ENNB 1 , 500 μg kg -1 FB 1 , 120 μg kg -1 ZEA.

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques: Tandem Mass Spectroscopy

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: LC-ESI-MS/MS chromatograms of mycotoxins from wheat extract spiked at 8 μg kg -1 for AFB 1 , 2 μg kg -1 for AFG 1 and AFB 2 , 1 μg kg -1 for AFG 2 , 100 μg kg -1 for 3-ADON, FB 2 and MON, 40 μg kg -1 for 15-ADON and NIV, 168 μg kg -1 for DON, 50 μg kg -1 for DON-3-G, 32.4 μg kg -1 for ENNA, 36 μg kg -1 for ENNA 1 , 28 μg kg -1 for ENNB, 30.4 μg kg -1 ENNB 1 , 500 μg kg -1 FB 1 , 120 μg kg -1 ZEA.

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques: Tandem Mass Spectroscopy

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: Method performance parameter in maize ( n = 3) for both of the compared methods.

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques:

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: Method performance parameter in wheat ( n = 3) for both of the compared methods.

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques:

Journal: Frontiers in Microbiology

Article Title: Development and Comparison of Two Multiresidue Methods for the Determination of 17 Aspergillus and Fusarium Mycotoxins in Cereals Using HPLC-ESI-TQ-MS/MS

doi: 10.3389/fmicb.2019.00361

Figure Lengend Snippet: Comparison between the certified (CC) and measured concentrations (MC) ( n = 3) of the certified maize and wheat reference material (Trilogy® Reference Material, Trilogy® Analytical Laboratory, Washington, MO, United States).

Article Snippet: Stock solutions of AFB 1 , AFB , AFG 1 , AFG , 3-ADON, 15-ADON, DON, DON-3-G, FB 1 , FB , in CH 3 CN/H O 50/50, v/v; MON, in CH 3 CN/H O 90/10, v/v; NIV and ZEA were purchased from Romer Labs Diagnostic GmbH (Tulln, Austria).

Techniques: Comparison

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: Basic properties of AFG-90H polymer.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: XRD patterns of Sm 2 O 3 , Sm 2 O 3 -APTES and Sm 2 O 3 -APTES/AFG-90H.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: SEM images of Sm 2 O 3 -APTES particles and morphology of Sm 2 O 3 -APTES/AFG-90H: ( a , b ) Sm 2 O 3 -APTES particles; ( c – h ) Sm 2 O 3 -APTES content: 0, 5, 10, 15, 20, and 30 wt%.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: Thermal performance curves: ( a ) TG; ( b ) DTG; ( c ) DSC and ( d ) T g of Sm 2 O 3 -APTES/AFG-90H.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: TG data for Sm 2 O 3 -APTES/AFG-90H (℃).

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: Mechanical properties of Sm 2 O 3 -APTES/AFG-90H: ( a ) Young’s modulus and elongation at break; ( b ) tensile strength; ( c ) Shore hardness.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques:

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: Shielding performance of Sm 2 O 3 -APTES/AFG-90H: ( a ) neutron permeability (I/I 0 ); ( b ) secondary γ dose.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques: Permeability

Journal: Polymers

Article Title: Influences of Modified Sm 2 O 3 on Thermal Stability, Mechanical and Neutron Shielding Properties of Aminophenol Trifunctional Epoxy Resin

doi: 10.3390/polym14030638

Figure Lengend Snippet: The decomposition temperature of different mass loss, tensile strength, neutron permeability of epoxy-based neutron shielding materials.

Article Snippet: X-ray diffraction (XRD) analyzed on the AFG-90H and Sm 2 O 3 particles were performed on Rigaku Ultima IV X-ray diffractometer from 10° to 80°.

Techniques: Permeability